Microcolumn High-Performance Liquid Chromatography

Paul Kucera0444422900, 9780444422903

Table of contents :
Microcolumn High-Performance Liquid Chromatography……Page 4
Contents……Page 6
Journal of Chromatography Library……Page 12
List of contributors……Page 14
Preface……Page 16
1. Introduction……Page 18
2. Instrument specifications……Page 19
3. Packed columns……Page 33
4. Open-tubular columns……Page 43
5. Packed capillary columns……Page 51
6. Conclusions……Page 52
7. References……Page 53
1. Introduction……Page 56
2. Factors affecting the design of a microbore liquid chromatograph……Page 57
3. Chromatographic apparatus……Page 69
4. Conclusions……Page 89
5. References……Page 90
1. Introduction……Page 92
2. Theory of time optimization……Page 95
3. Instrumental requirements……Page 107
4. Applications of high-speed analyses……Page 115
5. Summary and future trends……Page 125
6. References……Page 126
Foreword……Page 128
1. Coupling microbore columns……Page 129
2. Recycling microbore columns……Page 139
3. Differential frontal analysis……Page 151
4. Trace analysis and trace enhancement……Page 162
5. Summary……Page 167
6. References……Page 169
1. Introduction……Page 171
2 . Derivatization reagents……Page 173
3. Pre-column derivatization techniques……Page 174
4. Post-column derivatization techniques……Page 180
5. Applications……Page 189
6. Conclusions……Page 194
7. References……Page 195
1. Introduction……Page 196
2. Pharmaceuticals……Page 197
3. Miscellaneous biochemicals……Page 200
4. Nucleic acid constituents……Page 203
5. Industrial chemicals and miscellaneous extracts……Page 206
6. References……Page 210
1. Introduction……Page 211
2. Instrumental aspects……Page 214
3. Open-tubular columns……Page 234
4. Packed capillary columns……Page 250
5. Slurry-packed capillary columns……Page 257
6. Detectors for miniaturized columns……Page 263
7. References……Page 273
1. Introduction……Page 277
2. Developments in micro LC/MS coupling……Page 279
3. Sumnary……Page 314
4. Conclusion……Page 315
5. References……Page 316
Subject index……Page 318