Jack Cazes9780824721534, 0824721535
Table of contents :
b-Agonist Residues in Food, Analysis by LC……Page 74
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Acoustic Field-Flow Fractionation for Particle Separation……Page 80
Additives in Biopolymers, Analysis by……Page 82
Adhesion of Colloids on Solid Surfaces by……Page 86
Adsorption Chromatography……Page 89
Adsorption Studies by Field-Flow Fractionation……Page 93
Advances in Chiral Pollutants……Page 96
Affinity Chromatography with Immobilized Antibodies……Page 107
Affinity Chromatography: An Overview……Page 112
Aggregation of Colloids by Field-Flow Fractionation……Page 116
Alumina-Based Supports for……Page 119
Amino Acid Analysis by HPLC……Page 124
Amino Acids and Derivatives: Analysis by TLC……Page 128
Amino Acids, Peptides, and Proteins: Analysis by CE……Page 133
Analysis of Alcoholic Beverages by Gas Chromatography……Page 138
Analysis of Food Colors by Thin-Layer……Page 141
Analysis of Mycotoxins by TLC……Page 147
Analysis of Plant Toxins by TLC……Page 150
Analysis of Terpenoids by Thin-Layer Chromatography……Page 153
Analyte–Analyte Interactions, Effect on……Page 159
Antibiotics: Analysis by TLC……Page 164
Antioxidant Activity: An Adaptation for……Page 167
Application of Capillary Electrochromatography……Page 173
Applications of Evaporative Light-Scattering……Page 183
Applied Voltage: Effect on Mobility, Selectivity,……Page 185
Aqueous Two-Phase Solvent Systems……Page 186
Argon Detector……Page 190
Assessment of Lipophilicity by Reversed-Phase……Page 192
Asymmetric Flow FFF in Biotechnology……Page 197
Automation and Robotics in Planar Chromatography……Page 200
Axial Dispersion Correction Methods in GPC–SEC……Page 204
Band Broadening in Capillary Electrophoresis……Page 209
Band Broadening in Size-Exclusion Chromatography……Page 212
Barbiturates, Analysis by Capillary Electrophoresis……Page 217
Binding Constants: Determination……Page 224
Binding Molecules Via SH Groups……Page 227
Biopharmaceuticals by Capillary Electrophoresis……Page 229
Biopolymer Separations by……Page 233
Biotic Dicarboxylic Acids, CCC Separation with……Page 239
Bonded Phases in HPLC……Page 242
Buffer Systems for Capillary Electrophoresis……Page 246
Buffer Type and Concentration, Effect on Mobility, Selectivity,……Page 250
Calibration of GPC–SEC with Narrow……Page 253
Calibration of GPC–SEC with Universal……Page 256
Capacity……Page 259
Capillary Electrochromatography: An Introduction……Page 261
Capillary Electrophoresis and HPLC for Analysis of……Page 264
Capillary Electrophoresis in Nonaqueous Media……Page 272
Capillary Electrophoresis–Inductively Coupled……Page 275
Capillary Electrophoresis on Chips……Page 283
Capillary Electrophoresis: Introduction and Overview……Page 288
Capillary Isoelectric Focusing of Peptides,……Page 291
Capillary Isoelectric Focusing: An Overview……Page 295
Capillary Isotachophoresis……Page 298
Carbohydrates as Affinity Ligands……Page 300
Carbohydrates: Analysis by Capillary Electrophoresis……Page 304
Carbohydrates: Analysis by HPLC……Page 307
Carbohydrates: Analysis by TLC—New Visualization……Page 310
Catalyst Characterization by Reversed Flow……Page 312
CCC Solvent Systems……Page 317
CE–MS: Large-Molecule Applications……Page 320
Cell Sorting Using Sedimentation Field Flow Fractionation:……Page 323
Centrifugal Partition Chromatography: An Overview……Page 333
Centrifugal Precipitation Chromatography……Page 338
Ceramides: Analysis by Thin-Layer Chromatography……Page 341
Channeling and Column Voids……Page 345
Characterization of Metalloproteins……Page 346
Chelating Sorbents for Affinity Chromatography (IMAC)……Page 350
Chemometrics in Chromatography……Page 352
Chiral Chromatography by Subcritical……Page 358
Chiral Countercurrent Chromatography……Page 361
Chiral Separations by Capillary Electrophoresis……Page 364
Chiral Separations by GC……Page 369
Chiral Separations by HPLC……Page 371
Chiral Separations by Micellar Electrokinetic……Page 377
Chromatographic Methods Used to Identify and……Page 380
Classification of Organic Solvents……Page 399
Coil Planet Centrifuges……Page 401
Cold-Wall Effects in Thermal FFF……Page 414
Comprehensive Thermodynamic Approach to Ion……Page 416
Concentration Effects on Polymer Separation……Page 423
Concentration of Dilute Colloidal Samples……Page 427
Conductivity Detection in Capillary Electrophoresis……Page 431
Conductivity Detection in HPLC……Page 433
Congener-Specific PCB Analysis……Page 437
Copolymer Analysis by LC Methods,……Page 441
Copolymer Composition by GPC–SEC……Page 446
Copolymer Molecular Weights by GPC–SEC……Page 448
Coriolis Force in Countercurrent Chromatography……Page 450
Corrected Retention Time and Corrected……Page 452
Coumarins: Analysis by TLC……Page 453
Countercurrent Chromatographic Separation……Page 456
Countercurrent Chromatography–Mass Spectrometry……Page 461
Creatinine and Purine Derivatives, Analysis by HPLC……Page 465
Cross-Axis Coil Planet Centrifuge……Page 470
CZE of Biopolymers……Page 474
Dead Point (Volume or Time)……Page 479
Degassing of Solvents……Page 481
Dendrimers and Hyperbranched Polymers:……Page 483
Derivatization of Acids for GC Analysis……Page 487
Derivatization of Amines, Amino Acids,……Page 491
Derivatization of Analytes in Chromatography:……Page 495
Derivatization of Carbohydrates for GC Analysis……Page 499
Derivatization of Carbonyls for GC Analysis……Page 501
Derivatization of Hydroxy Compounds for GC Analysis……Page 505
Derivatization of Steroids for GC Analysis……Page 509
Detection (Visualization) of TLC Zones……Page 511
Detection in Countercurrent Chromatography……Page 514
Detection Methods in Field-Flow Fractionation……Page 517
Detection Principles……Page 522
Detector Linear Dynamic Range……Page 528
Detector Linearity and Response Index……Page 529
Detector Noise……Page 531
Displacement Chromatography……Page 533
Displacement Thin-Layer Chromatography……Page 536
Distribution Coefficient……Page 541
DNA Sequencing Studies by CE……Page 543
Drug Residues in Food, Detection/Confirmation by LC-MS……Page 547
Dry-Column Chromatography……Page 552
Dual Countercurrent Chromatography……Page 555
Dyes: Separation by Countercurrent Chromatography……Page 559
Eddy Diffusion in Liquid Chromatography……Page 562
Effect of Organic Solvents on Ion Mobility……Page 564
Effect of Temperature and Mobile Phase Composition……Page 567
Efficiency in Chromatography……Page 573
Efficiency of a Thin-Layer Chromatography Plate……Page 576
Electro-osmotic Flow……Page 583
Electro-osmotic Flow in Capillary Tubes……Page 587
Electro-osmotic Flow Nonuniformity: Influence……Page 592
Electrochemical Detection……Page 595
Electrochemical Detection in CE……Page 598
Electrokinetic Chromatography Including……Page 601
Electron-Capture Detector……Page 606
Electrospray Ionization Interface for CE–MS……Page 609
Eluotropic Series of Solvents for……Page 613
Elution Chromatography……Page 619
Elution Modes in Field-Flow Fractionation……Page 622
Enantiomer Separations by TLC……Page 626
Enantioseparation by Capillary Electrochromatography……Page 629
End Capping……Page 633
Enoxacin: Analysis by Capillary Electrophoresis and HPLC……Page 635
Environmental Applications of SFC……Page 641
Environmental Pollutants Analysis by……Page 645
Essential Oils Analysis by Gas Chromatography……Page 654
Evaporative Light Scattering Detection……Page 659
Exclusion Limit in GPC–SEC……Page 663
Extra-Column Dispersion……Page 664
Extra-Column Volume……Page 666
Fast Gas Chromatography……Page 668
Field-Flow Fractionation Data Treatment……Page 672
Field-Flow Fractionation Fundamentals……Page 675
Field-Flow Fractionation with Electro-osmotic Flow……Page 680
Flame Ionization Detector for GC……Page 683
Flavonoids, Analysis by Supercritical……Page 686
Flow Field-Flow Fractionation: Introduction……Page 690
Fluorescence Detection in Capillary Electrophoresis……Page 693
Fluorescence Detection in HPLC……Page 697
Foam Countercurrent Chromatography……Page 701
Focusing Field-Flow Fractionation……Page 705
Forensic Applications of Capillary Electrophoresis……Page 708
Forskolin Purification Using an Immunoaffinity Column……Page 713
Fraction Collection Devices……Page 716
Frit-Inlet Asymmetrical Flow Field-Flow Fractionation……Page 720
Frontal Chromatography……Page 722
Fronting of Chromatographic Peaks: Causes……Page 725
Gas Chromatography System Instrumentation……Page 727
Gas Chromatography–Mass Spectrometry Systems……Page 732
Golay Dispersion Equation……Page 739
GPC–SEC Analysis of Nonionic Surfactants……Page 741
GPC–SEC Viscometry from Multiangle Light Scattering……Page 744
GPC–SEC–HPLC Without Calibration: Multiangle Light……Page 747
GPC–SEC: Effect of Experimental Conditions……Page 752
GPC–SEC: Introduction and Principles……Page 754
Gradient Development in Thin-Layer Chromatography……Page 758
Gradient Elution……Page 762
Gradient Elution in Capillary Electrophoresis……Page 764
Gradient Elution: Overview……Page 766
Gradient Generation Devices and Methods……Page 770
Headspace Sampling……Page 774
Helium Detector……Page 776
High-Speed SEC Methods……Page 778
High-Temperature High-Resolution Gas Chromatography……Page 783
Histidine in Body Fluids, Specific Determination by HPLC……Page 787
HPLC Analysis of Amino Acids……Page 790
HPLC Analysis of Flavonoids……Page 797
HPLC Column Maintenance……Page 804
Hybrid Micellar Mobile Phases……Page 808
Hydrodynamic Equilibrium in CCC……Page 815
Hydrophilic Vitamins, Analysis by TLC……Page 818
Hydrophobic Interaction Chromatography……Page 823
Immobilized Metal Affinity Chromatography……Page 827
Immunoaffinity Chromatography……Page 830
Immunodetection……Page 834
Industrial Applications of CCC……Page 838
Influence of Organic Solvents on pKa……Page 841
Injection Techniques for Capillary Electrophoresis……Page 843
Inorganic Analysis by CCC……Page 846
Instrumentation of Countercurrent Chromatography……Page 851
Intrinsic Viscosity of Polymers: Determination by GPC……Page 855
Ion Chromatography Principles,……Page 858
Ion Exchange: Mechanism and Factors Affecting Separation……Page 862
Ion-Exchange Buffers……Page 866
Ion-Exchange Stationary Phases……Page 868
Ion-Exclusion Chromatography……Page 871
Ion-Interaction Chromatography……Page 874
Ion-Pairing Techniques……Page 878
Katharometer Detector for Gas Chromatography……Page 882
Kovats Retention Index System……Page 884
Large-Volume Injection for Gas Chromatography……Page 888
Large-Volume Sample Injection in FFF……Page 891
Laser-Induced Fluorescence Detection……Page 894
LC-NMR and LC-MS-NMR:……Page 901
Lewis Base–Modified Zirconia as……Page 914
Lipid Analysis by HPLC……Page 922
Lipid Classes: Purification by Solid-Phase Extraction……Page 927
Lipid Separation by Countercurrent Chromatography……Page 930
Lipids Analysis by Thin-Layer Chromatography……Page 938
Lipids Analysis by TLC……Page 942
Lipophilic Vitamins by Thin-Layer Chromatography……Page 947
Lipophilicity Determination of Organic Substances……Page 950
Lipoprotein Separation by Combined Use……Page 953
Liquid Chromatography–Mass Spectrometry……Page 956
Liquid–Liquid Partition Chromatography……Page 960
Long-Chain Polymer Branching: Determination by……Page 963
Longitudinal Diffusion in Liquid Chromatography……Page 966
Magnetic FFF and Magnetic SPLITT……Page 968
Mark–Houwink Relationship……Page 972
Mass Transfer Between Phases……Page 975
Metal-Ion Enrichment by Countercurrent Chromatography……Page 977
Metal-Ion Separation by Micellar High……Page 980
Metals and Organometallics: Gas Chromatography……Page 984
Metformin and Glibenclamide, Simultaneous……Page 988
Microcystin, Isolation by Supercritical Fluid Extraction……Page 994
Migration Behavior: Reproducibility……Page 999
Minimum Detectable Concentration (Sensitivity)……Page 1001
Mixed Stationary Phases in GC……Page 1002
Mobile Phase Modifiers for SFC: Influence on Retention……Page 1004
Molecular Interactions in GC……Page 1008
Molecular Weight and Molecular-Weight……Page 1010
Molecularly Imprinted Polymers……Page 1014
Monolithic Disk Supports for HPLC……Page 1020
Multidimensional TLC……Page 1027
Natural Products Analysis by CE……Page 1030
Natural Rubber: GPC–SEC Analysis……Page 1034
Neuropeptides and Neuroproteins……Page 1036
Neurotransmitter and Hormone Receptors:……Page 1040
Nitrogen /Phosphorus Detector……Page 1042
Nonionic Surfactants: GPC–SEC Analysis……Page 1044
Normal-Phase Chromatography……Page 1047
Normal-Phase Stationary Packings……Page 1050
Nucleic Acids, Oligonucleotides, and DNA:……Page 1054
Octanol–Water Partition Coefficients by CCC……Page 1058
On-Column Injection for GC……Page 1061
Open-Tubular (Capillary) Columns……Page 1066
Open-Tubular and Micropacked Columns……Page 1069
Optical Activity Detectors……Page 1073
Optical Quantification (Densitometry) in TLC……Page 1076
Optimization of Thin-Layer Chromatography……Page 1081
Organic Acids, Analysis by Thin Layer Chromatography……Page 1085
Organic Extractables from Packaging Materials:……Page 1091
Overpressured Layer Chromatography……Page 1103
Packed Capillary Liquid Chromatography……Page 1106
Particle Size Determination by Gravitational FFF……Page 1109
Peak Identification with a Diode Array Detector……Page 1114
Peak Purity Determination with a Diode Array Detector……Page 1121
Peak Skimming for Overlapping Peaks……Page 1126
Pellicular Supports for HPLC……Page 1128
Penicillin Antibiotics in Food: Liquid……Page 1131
Peptide Analysis by HPLC……Page 1136
Peptide Separation by Countercurrent Chromatography……Page 1140
Pesticide Analysis by Gas Chromatography……Page 1146
Pesticide Analysis by Thin-Layer Chromatography……Page 1149
pH, Effect on MEKC Separation……Page 1153
pH-Peak-Focusing and pH-Zone-Refining……Page 1156
Pharmaceuticals: Analysis by TLC……Page 1162
Phenolic Acids in Natural Plants: Analysis by HPLC……Page 1165
Phenolic Compounds, Analysis by HPLC……Page 1174
Phenolic Drugs, New Visualizing Reagents……Page 1183
Phenols and Acids: Analysis by TLC……Page 1191
Photodiode-Array Detection……Page 1195
Photophoretic Effects in FFF of Particles……Page 1199
Plant Extracts: Analysis by TLC……Page 1202
Plate Number, Effective……Page 1205
Plate Theory……Page 1207
Pollutant–Colloid Association by Field-Flow……Page 1210
Pollutants in Water by HPLC……Page 1214
Polyamide Analysis by GPC–SEC……Page 1218
Polycarbonates: GPC–SEC Analysis……Page 1222
Polyester Analysis by GPC–SEC……Page 1225
Polymer Additives: Analysis by……Page 1228
Polymer Degradation in GPC–SEC Columns……Page 1231
Polymerase Chain Reaction Products:……Page 1234
Polynuclear Aromatic Hydrocarbons in Environmental……Page 1239
Porous Graphitized Carbon Columns in……Page 1244
Potential Barrier Field-Flow Fractionation……Page 1254
Preparative HPLC Optimization……Page 1257
Preparative TLC……Page 1262
Procyanidin Separation by CCC with……Page 1265
Programmed Flow Gas Chromatography……Page 1268
Programmed Temperature Gas Chromatography……Page 1271
Prostaglandins: Analysis by HPLC……Page 1273
Protein Analysis by HPLC……Page 1277
Protein Immobilization……Page 1282
Protein Separations by Flow Field-Flow Fractionation……Page 1286
Proteins as Affinity Ligands……Page 1290
Purge-Backflushing Techniques in Gas Chromatography……Page 1293
Purification of Cyanobacterial Hepatotoxin……Page 1300
Purification of Peptides with Immobilized Enzymes……Page 1307
Pyrolysis–Gas Chromatography–Mass Spectrometry……Page 1310
Quantitation by External Standard……Page 1314
Quantitation by Internal Standard……Page 1316
Quantitation by Normalization……Page 1318
Quantitation by Standard Addition……Page 1319
Quantitative Structure–Retention Relationship……Page 1321
Quinolone Antibiotics in Food, Analysis by LC……Page 1325
Radiochemical Detection……Page 1328
Radius of Gyration Measurement by GPC–SEC……Page 1331
Rate Theory in Gas Chromatography……Page 1334
Refractive Index Detector……Page 1336
Resin Microspheres as Stationary Phase for……Page 1339
Resolution in HPLC: Selectivity, Efficiency, and Capacity……Page 1346
Resolving Power of a Column……Page 1349
Response Spectrum in Chromatographic Analysis……Page 1351
Retention Factor: Effect on MEKC Separation……Page 1366
Retention Gap Injection Method……Page 1368
Retention Time and Retention Volume……Page 1370
Reversed-Phase Chromatography:……Page 1371
Reversed-Phase Stationary Phases……Page 1375
Rf……Page 1379
Rotation Locular Countercurrent Chromatography……Page 1381
Sample Application in TLC……Page 1384
Sample Preparation……Page 1391
Sample Preparation and Stacking……Page 1394
Sample Preparation Prior to HPLC……Page 1398
Scale-up of Countercurrent Chromatography……Page 1415
SEC with On-Line Triple Detection: Light Scattering,……Page 1419
Sedimentation Field-Flow Fractionation of Living Cells……Page 1424
Selection of a Gradient HPLC System……Page 1430
Selection of an Isocratic HPLC System……Page 1438
Selectivity……Page 1446
Selectivity: Factors Affecting,……Page 1449
Separation of Alkaloids by Countercurrent Chromatography……Page 1452
Separation of Antibiotics……Page 1457
Separation of Chiral Compounds……Page 1462
Separation of Flavonoids by……Page 1466
Separation of Metal Ions by Centrifugal……Page 1470
Separation Ratio……Page 1474
Sequential Injection Analysis in HPLC……Page 1475
Settling Time of Two-Phase Solvent Systems……Page 1479
Silica Capillaries: Chemical Derivatization……Page 1482
Silica Capillaries: Epoxy Coating……Page 1486
Silica Capillaries: Polymeric Coating……Page 1489
Silver Ion TLC of Fatty Acids……Page 1492
Size Separations by Capillary Electrophoresis……Page 1495
Solute Focusing Injection Method……Page 1500
Solute Identification in TLC……Page 1502
Solvent Effects on Polymer Separation by ThFFF……Page 1506
Spacer Groups for Affinity Chromatography……Page 1509
Spiral Disk Assembly: An Improved Column Design for……Page 1511
Split /Splitless Injector……Page 1522
Stationary Phases for Packed Column……Page 1523
Stationary-Phase Retention……Page 1527
Steroid Analysis by Gas Chromatography……Page 1531
Steroid Analysis by TLC……Page 1536
Supercritical Fluid Chromatography……Page 1540
Supercritical Fluid Chromatoraphy……Page 1543
Supercritical Fluid Chromatography……Page 1546
Supercritical Fluid Chromatography: An Overview……Page 1549
Supercritical Fluid Extraction……Page 1553
Surface Phenomena in Sedimentation FFF……Page 1556
Surfactants: Analysis by HPLC……Page 1559
Synergistic Effects of Mixed Stationary……Page 1562
Systematic Selection of Solvent Systems for……Page 1565
Taxanes Analysis by HPLC……Page 1572
Taxines Analysis by HPLC……Page 1579
Taxoids Analysis by TLC……Page 1585
Temperature Program: Anatomy……Page 1588
Temperature: Effect on MEKC Separation……Page 1589
Temperature: Effects on Mobility, Selectivity,……Page 1591
Terpenoids, Separation by HPLC……Page 1593
Theory and Mechanism of Thin-Layer Chromatography……Page 1596
Thermal FFF of Polymers and Particles……Page 1601
Thermal FFF of Polystyrene……Page 1605
Thermal FFF: Basic Introduction and Overview……Page 1607
Thermodynamics of GPC–SEC Separation……Page 1610
Thermodynamics of Retention in Gas Chromatography……Page 1613
Thin-Layer Chromatographic Study of Quantitative……Page 1614
Thin-Layer Chromatography of Natural Pigments……Page 1617
Thin-Layer Chromatography of Synthetic Dyes……Page 1620
Thin-Layer Chromatography–Mass Spectrometry……Page 1623
Three-Dimensional Effects in Field-Flow……Page 1627
TLC Immunostaining of Steroidal Alkaloid Glycosides……Page 1630
TLC Sandwich Chamber……Page 1633
TLC Sorbents……Page 1636
Topological Indices, Use in HPLC……Page 1641
Trace Enrichment……Page 1651
Troubleshooting HPLC Instrumentation……Page 1654
Two-Dimensional Thin-Layer Chromatography……Page 1667
Ultrathin-Layer Gel Electrophoresis……Page 1671
Unified Chromatography……Page 1676
Uremic Toxins in Biofluids, Analysis by HPLC……Page 1679
Validation of HPLC Instrumentation……Page 1690
Validation of TLC Analyses……Page 1706
van’t Hoff Curves……Page 1709
Vinyl Pyrrolidone Homopolymer……Page 1711
Viscometric Detection in GPC–SEC……Page 1714
Vitamin B12 and Related Compounds in Food,……Page 1718
Void Volume in Liquid Chromatography……Page 1723
Weak Affinity Chromatography……Page 1725
Wheat Protein by Field-Flow Fractionation……Page 1728
Whey Proteins, Anion-Exchange Separation……Page 1731
Zeta-Potential……Page 1736
Zirconia–Silica Stationary Phases for HPLC:……Page 1738
Zone Dispersion in Field-Flow Fractionation……Page 1749
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